High Temperature Synthesis and Crystal Growth

The High Temperature Synthesis and Crystal Growth Laboratory is a unique facility for preparation and single crystal growth of inorganic materials, able to handle uranium and thorium. It includes several melting techniques (like arc-melting or induction-melting), high-temperature crystal growth methods (as Czochralski, Bridgman, Floating Zone or Flux), Hot-press processing, Splat Cooling/Melt Spinning for metallic glasses/nanograined materials, and also Electrospinning for micra/submicra fibers production. This laboratory has been supporting national and international projects, either in the framework of projects participated by the Solid-State Group, or by demand of other researchers inside and outside IST.

Main equipment:

Induction furnace equipped with cold crucibles and accessories for the growth of single crystals by the Czochralski, Bridgman and Floating Zone methods.

  • Arc furnaces.
  • Resistive furnaces (up to 2200 C).
  • Two-zone furnaces (up to 1100ºC).
  • Flux equipment (up to 1400º).
  • Splat Cooling System.
  • Melt Spinning System.
  • Electrospinning System.
  • Laboratory precision cut-off machine for small dimension materials.
  • Low damage spark erosion unit.

Contact Person at IST: António Pereira Gonçalves – apg@ctn.tecnico.ulisboa.pt

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